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I did this on a small scale all the time.

Rather than running it in a 10mL round bottom, just use a 25 mL vial. You can fit a rubber septum and purge it. Magnetic stir bars are small enough to fit. You can add reagents using a syringe.

Then just rinse and toss after.

Quality glassware isn’t cheap because the ground glass joint has to be precisely ground to not leak. But if you don’t need a condenser or drop funnel, disposable vials work just fine.



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